He also accused the international community of not doing enough to ease the suffering of the Syrian people, condemning its "inability to enforce resolutions, in particular regarding humanitarian issues, (such as) the lifting of sieges, access to aid, the release of prisoners and adherence to the ceasefire".
The regime and non-jihadist rebels agreed a shaky ceasefire in February to bolster the peace talks but repeated violations have left the truce hanging by a thread.
"The endless negotiations are harming the fate of the Syrian people," Alloush added. "I therefore announce my withdrawal from the delegation and my resignation" from the main opposition High Negotiations Committee (HNC).
The last round of peace talks in Geneva reached a deadlock in April when the HNC suspended its participation over an escalation of fighting on the ground.
A new round of talks had been expected for the end of May, but no new date has been announced.
The UN's peace envoy for Syria, Staffan de Mistura, on Thursday said he had no plans to convene another round in the next two or three weeks.
Diplomats have said there was little chance that the opposition would take part in new peace talks if violence was raging and no aid was reaching civilians.
The talks aim to reach a political settlement to end the five-year war that has left 280,000 dead and driven millions from their homes.
The fate of Assad has been a key stumbling block in the negotiations, with the opposition insisting any peace deal must include his departure while Damascus says his future is non-negotiable.
On the ground in Syria meanwhile, thousands of civilians fled a fresh offensive by the Islamic State group in the north, the Syrian Observatory for Human Rights said Sunday.
The shock offensive against the towns of Marea and Azaz threatens to overrun the last swathe of territory in the east of Aleppo province held by non-jihadist rebels.
Further east, US-led coalition warplanes targeted IS positions north of Raqa, killing 45 IS fighters, the Observatory said.
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The regime and non-jihadist rebels agreed a shaky ceasefire in February to bolster the peace talks but repeated violations have left the truce hanging by a thread.
"The endless negotiations are harming the fate of the Syrian people," Alloush added. "I therefore announce my withdrawal from the delegation and my resignation" from the main opposition High Negotiations Committee (HNC).
The last round of peace talks in Geneva reached a deadlock in April when the HNC suspended its participation over an escalation of fighting on the ground.
A new round of talks had been expected for the end of May, but no new date has been announced.
The UN's peace envoy for Syria, Staffan de Mistura, on Thursday said he had no plans to convene another round in the next two or three weeks.
Diplomats have said there was little chance that the opposition would take part in new peace talks if violence was raging and no aid was reaching civilians.
The talks aim to reach a political settlement to end the five-year war that has left 280,000 dead and driven millions from their homes.
The fate of Assad has been a key stumbling block in the negotiations, with the opposition insisting any peace deal must include his departure while Damascus says his future is non-negotiable.
On the ground in Syria meanwhile, thousands of civilians fled a fresh offensive by the Islamic State group in the north, the Syrian Observatory for Human Rights said Sunday.
The shock offensive against the towns of Marea and Azaz threatens to overrun the last swathe of territory in the east of Aleppo province held by non-jihadist rebels.
Further east, US-led coalition warplanes targeted IS positions north of Raqa, killing 45 IS fighters, the Observatory said.
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